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Model studies for the synthesis of galbonolide B

journal contribution
posted on 2023-06-07, 22:05 authored by James Eshelby, Matthias Goessmann, Philip J Parsons, Lewis Pennicott, Adrian Highton
The construction of the fourteen membered ring present in galbonolide B 1 is reported. The 10,11-diene system present in the southern portion of 1 has been constructed using an ester enolate rearrangement/ silicon mediated fragmentation cascade, whilst the macrocycle has been synthesised following a Johnson rearrangement/ mercury assisted ring closure protocol.

History

Publication status

  • Published

Journal

Organic and Biomolecular Chemistry

ISSN

1477-0520

Publisher

Royal Society of Chemistry

Issue

16

Volume

3

Page range

2994-2997

Pages

4.0

Department affiliated with

  • Chemistry Publications

Notes

Synthetic work carried at Sussex and directed by the principle author PJP also involved, two industrial collaborators as co authors. A novel approach to the synthesis of galbonolide B.

Full text available

  • No

Peer reviewed?

  • Yes

Legacy Posted Date

2012-02-06

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