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Microwave-mediated synthesis of N-methyliminodiacetic acid (MIDA) boronates

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posted on 2023-06-08, 20:40 authored by Adam J Close, Paul Kemmitt, Matthew K Emmerson, John SpencerJohn Spencer
A library of over 20, mainly aryl or heteroaryl, N-methyliminodiacetic acid (MIDA) boronates have been synthesised. A rapid microwave-mediated (MW) method (5–10 min) has been developed using polyethylene glycol 300 (PEG 300) as solvent. However, acetonitrile (MeCN) and dimethylformamide (DMF) were found to be alternative solvents, the latter especially for 2-substituted aryl boronic acids.

History

Publication status

  • Published

File Version

  • Accepted version

Journal

Tetrahedron

ISSN

0040-4020

Publisher

Elsevier

Issue

47

Volume

70

Page range

9125-9131

Department affiliated with

  • Chemistry Publications

Full text available

  • Yes

Peer reviewed?

  • Yes

Legacy Posted Date

2015-05-01

First Open Access (FOA) Date

2015-05-01

First Compliant Deposit (FCD) Date

2015-05-01

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